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HPLC法测定复&#21

 
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lin91957
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PostPosted: Thu 21:09, 17 Mar 2011    Post subject: HPLC法测定复&#21
HPLC法测定复合维生素注射液（13种）中4种脂溶性维生素的含量
。而在洗脱时也应严格控制洗脱速度，通过试验发现流速大于1．0ml·min时，维生素D峰面积较小，流速小于1．0ml·min时，维生素D，峰与其他杂峰的分离度不理想。因此在对样品进行萃取时，应将样品在SPE小柱上处理2次，在进行洗脱时，应将洗脱速度控制在1．0ml·rain～。
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