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反相高效液

 
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lin91957
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PostPosted: Thu 8:28, 17 Mar 2011    Post subject: 反相高效液

反相高效液相色谱法测定色甘酸钠滴鼻液的含量
。2.7样品测定取色甘酸钠滴鼻液1.0ml,置50rnJ量瓶中,以流动相稀释至刻度,摇匀,进样20l,记录峰面积,代人回归方程计算含量,并同时与UV法[1]比较,结果见表3。表3样品测定结果(标示量)3讨论UV法测得的结果偏高,可能是色甘酸钠分解产物的干扰所致[。本文所建立的RP—HPLC法操作简便、结果准确、重复性好,适用于色甘酸钠滴鼻液含量的测定。
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